Equipment

Bruker AVANCE NEO 600 MHz NMR spectrometer

• Magnet System Ascend™ 600 MHz / 54 mm (14.09 T)
• 3 RF channels
• 5 mm BBO CryoProbe Prodigy (BB-H&F-D) with N2 cooled electronics, z-gradient (60 G/cm at the probe), temp range: -40°C ¸ +150°C. Enhanced sensitivity for both 1H and X nuclei, for analysis of low concentration samples.
• 5 mm iTBO triple resonance broadband probehead (BBF/H/F/D) with capacity for simultaneous ¹H and ¹⁹F decoupling of X nuclei, z-gradient (50 G/cm at the probe), temp range: -150°C ¸ +150° Particularly suitable for the analysis of fluorinated compounds in pharmaceutical, polymer and biological research.
• Automated tuning & matching (ATM) for both probeheads
• Gradient control unit and 10A gradient amplifier
• Temperature control system (BSVT) and BCU-II cooling unit, VT measurements: -170°C ¸ +250°C
• Automatic sample changer SampleCase Plus for 60 samples
• Home made module for in situ irradiation of the samples inside the NMR spectrometer

Applications:

• Multidimentional NMR experiments for investigation of liquid state samples with various research applications including metabolomics, pharmaceuticals, natural products research, complex mixtures, biomolecules, molecular structure and interactions, photosensitive reactions, etc.

Bruker AVANCE NEO 400 MHz NMR spectrometer

• Magnet System Ascend™ 400 MHz / 54 mm (9.4 T)
• 3 RF channels
• 5 mm iTBO triple resonance broadband probehead (BBF/H/F/D) with capacity for simultaneous ¹H and ¹⁹F decoupling of heteronuclei, z-gradient (50 G/cm at the probe), temp range: -150°C  +150°C.
• 5 mm iProbe BBFO BBF/1H (Smart Probe), for direct and indirect detection experiments, broadband channel tunable from 15N to 19F.
• Automated tuning & matching (ATM) for both probes
• Gradient control unit and 10A gradient amplifier
• Temperature control system (BSVT) and BCU-I cooling unit, VT measurements: -170°C ¸ +250°C
• Automatic sample changer SampleCase for 24 samples

Applications:

• For routine high throughput measurements in liquid state
• Service analyses for academic and industrial users
• Education and teaching of junior researchers and students

Bruker Avance III HD 600 MHz spectrometer

• Ultrashield^TM magnet D 262/54 (09 T).

Solid state NMR equipment:

• Solid state 4mm iProbe CPMAS DR-H&F VTN – (latest generation), MAS 15 kHz, frequency range: ¹H, ¹⁹F and X-nuclei ³¹P to ¹⁵N, with automatic tuning&matching, and automatic magic angle adjustment; temp. range: -80°C ¸ +200°C;

Applications: wide range of applications in materials research (organic solids, pharmaceuticals, catalysts etc.), in automated workflow

• Solid state 1.3 mm CPMAS (X/F-H DVT) double resonance probehead, frequency range: ¹H, ¹⁹F and X-nuclei from ³¹P to ¹⁵N; MAS speed up to 67 kHz; temp range: -30°C ¸ +70°C;

Applications: suitable for NMR study of reasonably sensitive nuclei with large chemical shift anisotropies or quadrupole broadenings that can be averaged under fast MAS (²³Na, ²⁷Al, etc.)

• MAS III unit

NMR equipment for investigation of soft and semisolid materials:

• 5 mm Broadband Diffusion Probe (DIFF-DR-BB/1H&19F-D-Z-5mm), frequency range: ¹H, ¹⁹F and X-nuclei ³¹P to ¹⁵N, temp range: -40°C ¸ +150°C; high gradient amplifier (60 A) and z-gradients of 1700 G/cm at the probe;

Applications: suitable for investigation of molecular transport phenomena (translational diffusion) in complex colloid systems with large particles and high viscosity;

• 4mm triple resonance ¹H/¹³C/³¹P high resolution magic angle spinning (15 kHz) probehead (HR-MAS) with gradients along the magic angle (50 G/cm at the probe), temp range: -20°C ¸ 80°C;

Applications: for investigation of polymeric (hydro)gels, semi-solid samples and phenomena at solid-liquid interfaces

Liquid phase NMR equipment:

• 5 mm direct dual probehead (BBO) ³¹P – ¹⁰⁹Ag/¹H, with actively shielded Z-gradients and automatic tuning and matching accessory (ATMA).
• Automatic sample changer B-ACS for 60 samples.
• Temperature control unit – B-VT 3000 with temperature range 150 ¸ 390 K
• 5 mm inverse triple probehead (TBI) ¹H/³¹P – ¹⁰⁹Ag/¹³C with actively shielded Z-gradients
• Home made module for in situ irradiation of the samples inside the NMR spectrometer

Applications: for structural analysis and stereochemistry of synthetic organic compounds, investigation of tautomeric and conformational equilibria, chemical profiling and metabolic analysis of food and natural products

Bruker Avance DRX 250

• Magnet 131/52 (87T).
• Two radio frequency channels with liner amplifier BLAXH40.
• 5 mm direct dual probehead (BBO) ³¹Р – ¹⁰⁹Ag/¹H with actively shielded Z-gradients.
• 5 mm quattro probehead (QNP) ¹Н, ¹³С, ³¹Р, ¹⁹F with actively shielded Z-gradients.
• 5 mm dual probeheads ¹H/¹³
• 10 mm direct broadband probeheads ³¹Р – ¹⁵N/¹
• 10 mm direct broadband probeheads ¹⁵N – ¹⁰⁹Ag/¹
• Gradient unit GRASPII (10A).
• Automatic sample changer Sample Xpress for 60 samples.
• Temperature unit – B-VT 2000 with temperature range 170 ¸ 450 K.